کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1461216 989617 2014 8 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Fast synthesis of NaNbO3 and K0.5Na0.5NbO3 by microwave hydrothermal method
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
Fast synthesis of NaNbO3 and K0.5Na0.5NbO3 by microwave hydrothermal method
چکیده انگلیسی

Synthesis of sodium and potassium–sodium niobates (NaNbO3 and K0.5Na0.5NbO3) was achieved by reducing the reaction time via microwave-assisted hydrothermal route. Sodium niobate was synthesized at 180 °C for 15 min using NaOH 6 M. During the synthesis of KNN at 180 °C, the K4Na4Nb6O19–9H2O intermediate phase appeared. By increasing the temperature to 200 and 220 °C, the pure KNN phase was obtained. Potassium–sodium niobate was prepared at 220 °C for 15 min using KOH/NaOH 8 and 10 M. These results were confirmed by X-ray diffraction, Scanning Electron Microscopy and Raman spectroscopy. The NaNbO3 and K0.5Na0.5NbO3 powders consisted of agglomerated pseudo-cubic crystals.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 40, Issue 9, Part B, November 2014, Pages 14757–14764
نویسندگان
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