کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1461972 | 989625 | 2012 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis of nanocrystalline cerium oxide by high energy ball milling
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
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چکیده انگلیسی
We have synthesized pure nanocrystalline CeO2 powders of nearly spherical shape using high-energy attritor ball mill. Milling parameters such as the milling speed of 400 rpm, ball to powder ratio (40:1), milling time (30 h) and water cooled media were determined to be suitable for synthesizing nanosize (∼10 nm) powders of CeO2. The powders after milling for various durations (up-to 50 h) were characterized by X-ray Diffraction, Scanning Electron Microscopy, Energy-dispersive X-ray Spectrometry and Transmission Electron Microscopy. An average particle size of 10 nm was obtained at 30 h milling, after which the particle agglomeration started, and a mixture of nanocrystalline and amorphous phase was observed after 50 h milling.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 38, Issue 7, September 2012, Pages 5783–5789
Journal: Ceramics International - Volume 38, Issue 7, September 2012, Pages 5783–5789
نویسندگان
T.P. Yadav, O.N. Srivastava,