کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1463755 | 989651 | 2012 | 7 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Stereometric analysis of nanostructured boehmite coatings synthesized by aluminum nitride powder hydrolysis Stereometric analysis of nanostructured boehmite coatings synthesized by aluminum nitride powder hydrolysis](/preview/png/1463755.png)
We studied the morphological properties of precipitated, nanostructured, boehmite coatings on a polished alumina surface by exploiting the aluminum nitride (AlN) powder hydrolysis at elevated temperatures. The hydrolysis tests of the 3 wt% AlN powder suspensions in the temperature range 50–90 °C were performed in order to estimate the time needed for the synthesis of the coatings. They consisted of interlocked boehmite lamellas, positioned perpendicularly to the ceramic surface, and they exhibited a strong temperature-dependent size and surface density. The aim of this research was a quantitative assessment of the as-formed boehmite coatings. Based on electron microscopy micrographs, a stereometric analysis of the as-prepared coatings was performed in order to estimate the relevant geometric parameters of the lamellas. In spite of the temperature-dependent lamellas’ size and surface density, the specific volume of the coatings was similar for all the synthesis temperatures.
Journal: Ceramics International - Volume 38, Issue 6, August 2012, Pages 4853–4859