کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1464428 989661 2009 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Synthesis and characterization of boehmitic alumina coated graphite by sol–gel method
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
Synthesis and characterization of boehmitic alumina coated graphite by sol–gel method
چکیده انگلیسی

Non-wettability property makes graphite a good protecting material against the molten metal and/or slag. Properties like high oxidation potential between 600 and 1200 °C and non-wettability with water at room temperatures limits the usage of graphite in castable refractory applications. In this study, sol–gel method, which is a relatively cheaper process, was used. Boehmitic sol was obtained by hydrolyzing and peptiziting the alkoxide AIP (aluminum isopropoxide) used as alumina source. Then natural flake graphite was mixed with the boehmitic solution for coating of graphite. At 120 °C boehmitic sol coated graphite was dried and gelled. Then heat threaded at 550 °C for γ-Al2O3 transformation of boehmite. Products that obtained from the studies were characterized with FTIR and XRD tests. Alumina coated graphite samples were made by repeating the same steps and TG analysis were made to investigate the oxidation behaviour of the samples. Finally, SEM–EDS analyses were carried out to investigate the microscopic properties of the alumina coated graphite powders.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 35, Issue 5, July 2009, Pages 2029–2034
نویسندگان
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