کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1489346 | 992306 | 2012 | 4 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Synthesis and characterization of iron orthophosphate by solution combustion method Synthesis and characterization of iron orthophosphate by solution combustion method](/preview/png/1489346.png)
The present work applies solution combustion synthesis (SCS) by employing glycine as organic fuel to stimulate the synthesis of pure iron orthophosphate with well-defined reaction parameters. The structural and morphological properties of the products were characterized and confirmed by powder X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) and surface analyzer, respectively. Thermal behaviors were also investigated by TG/DT analyses. The optimal condition was set at 500 °C in a few minutes, giving pure iron orthophosphate with a good level of crystallinity and 11,769 m2/g surface area. The results proved SCS a time saving and practically applicable method.
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► Solution combustion synthesis was firstly employed to prepare FePO4.
► Pure, well-crystallized and porous FePO4 was obtained and characterized.
► The results proved SCS a time saving and practically applicable method.
Journal: Materials Research Bulletin - Volume 47, Issue 12, December 2012, Pages 4013–4016