کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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1504515 | 1510995 | 2014 | 4 صفحه PDF | دانلود رایگان |
Hydrothermal method synthesis of α-MnO2 nanowires has been achieved at different temperatures in this work. X-ray diffraction and transmission electron microscopy confirmed the pure phase of the α-MnO2 nanowires. All of the samples crystallized in a single-phase nanowires shape. The α-MnO2 nanowires diameter increased from 11 nm to 21 nm with the increase in hydrothermal temperature from 120 °C to 200 °C. The α-MnO2 catalytic activity on the decomposition of ammonium perchlorate (AP) was characterized through thermogravimetric analysis. The decomposition rate of AP with the addition of α-MnO2 was size relative. The 11 nm MnO2 nanowires exhibited the best catalytic activity, which lowered the high-temperature peak of AP by 130 °C.
With reducing diameter, α-MnO2 nanowires showed enhanced catalytic activities in thermal decomposition of ammonium perchlorate.Figure optionsDownload as PowerPoint slide
Journal: Solid State Sciences - Volume 27, January 2014, Pages 69–72