کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1504999 | 993749 | 2012 | 5 صفحه PDF | دانلود رایگان |

The new hydrogen bonding single crystal of 3-hydroxyanilinium-2,5-dimethylbenzenesulphonate (3HADB) complex has been synthesized and grown by slow evaporation solution growth technique. The grown crystal was confirmed by single crystal X-ray diffraction, Fourier Transform Infrared (FT-IR) and proton Nuclear Magnetic Resonance (1HNMR) spectral studies. Single crystal X-ray diffraction study shows that 3HADB crystallizes in the orthorhombic crystal system with noncentrosymmetric Pna21 space group. The title compound was characterized by UV–Vis–NIR absorption and TG/DTA thermal analysis studies. The second harmonic generation efficiency of powdered 3HADB was determined by Kurtz and Perry method.
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► The new single crystal of 3HADB complex has been grown from saturated solution.
► 3HADP crystallize orthorhombic system with Pna21 noncentrosymmetric space group.
► Powder test of Kurtz–Perry method shows SHG conversion.
Journal: Solid State Sciences - Volume 14, Issue 8, August 2012, Pages 1141–1145