Metallurgical investigation of the aging process on tensile fracture welded joints in pipeline steel

The effects of aging in the tensile fracture behavior of welded joints of API5L-X52 pipe steel were studied by accelerating aging at 250 °C for different periods of time. The weld metal, heat affected zone and base metal, showed an increase in yield strength while the strain-hardening exponent decreased at early stages of aging. A maximum strength and minimum hardening exponent was found at 500 h due to peak-aging. Subsequently, both properties exhibited an opposite behavior due to over-aging. Tensile fractured specimens for the three different zones exhibited ductile failure, presenting microvoid morphology associated with the coalescence of microcavities. An increase in void density and a reduction in diameter during short periods in the fractured specimens were observed. The maximum density and minimum diameter of voids were obtained at 500 h and were linked to the improvement of strength and precipitation of nanoparticles. Afterward, the fractured surfaces exhibited a reduction in density and the diameters of voids were larger, having been induced by the deterioration of strength and coarsening of particles.