کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1678050 1009926 2010 9 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
The GIF Quantum, a next generation post-column imaging energy filter
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
The GIF Quantum, a next generation post-column imaging energy filter
چکیده انگلیسی

We describe a new post-column imaging energy filter for (scanning) transmission electron microscopy from 60 to 300 kV operating voltage. The completely redesigned GIF quantum has a gradient magnetic prism, dodecapole optics, a 10-times faster 40 Mpixel/sec CCD camera, a 1 μs electrostatic shutter, and new user interface, control, and auto-alignment software. An 8 dodecapole lens system, performs full 2nd and 3rd, and partial 4th and 5th order aberration correction. The improved aberration correction has allowed the size of the entrance aperture to be nearly doubled to 9.0 mm compared to current generation post-column designs. The electrostatic shutter provides exposure control down to 1 μs, extending the exposure time range to over 7 orders of magnitude. Spectroscopy operation has been improved with a larger 2 keV field of view at 200 kV, and a maximum acquisition rate of 1000 spectra per second. A high-speed DualEELS mode simultaneously acquires core- and low-loss spectra up to 2 keV apart. A more intuitive user interface includes new capabilities such as automated exposure control and optimized full spectrum acquisition. The auto-alignment software has been significantly enhanced to use the full flexibility of the dodecapole lens system.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultramicroscopy - Volume 110, Issue 8, July 2010, Pages 962–970
نویسندگان
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