کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1678894 | 1009975 | 2007 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Effects of 10Â MeV electron irradiation at high temperature of a Ni-Mo-based Hastelloy
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A Hastelloy alloy was irradiated with 10 MeV electrons at 650 °C for 700 h to a total dose of 2Ã10â3 displacements per atom (dpa). The microstructure of irradiated and non-irradiated specimens of this alloy were investigated by transmission electron microscopy (TEM). The non-irradiated specimens were analyzed by 3-D atom probe tomography (APT) in a local-electrode atom-probe (LEAPâ¢). TEM analysis before the irradiation detects small precipitates with a mean diameter of 22 nm, which are coherent with the FCC matrix. The number density of these precipitates is â¼7Ã1018 mâ3. Electron diffraction patterns from these precipitates exhibit superlattice reflections corresponding to the L12 ordered structure. The chemical composition of the precipitates, as measured by APT, is around 75 at% Ni with additions of Al, Ti and Mo. After electron irradiation, small precipitates with an irregular morphology are observed. The number density of these new precipitates about 1020 mâ3 is greater than that of the L12 ordered precipitates before irradiation. The L12 superlattice reflections disappear completely, instead diffuse diffraction spots are observed at ã1120ãFCC, which is attributed to compositional short-range order (SRO). The results are discussed with respect to the influence of the electron irradiation on the morphology and structure of the ordered precipitates.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultramicroscopy - Volume 107, Issue 9, September 2007, Pages 786-790
Journal: Ultramicroscopy - Volume 107, Issue 9, September 2007, Pages 786-790
نویسندگان
N. Wanderka, A. Bakai, C. Abromeit, D. Isheim, D.N. Seidman,