Obtaining full contact for measuring polydimethylsiloxane mechanical properties with flat punch nanoindentation

Procedure to establish full contact between the sample and the 1 mm diameter cylindrical flat punch tip to measure polydimethylsiloxane (PDMS) mechanical properties using the Hysitron TriboIndenter is described. This procedure differs from the standard automated indentation because each indent has to be performed manually after establishing full contact with the sample surface. Incomplete contact happens because of the sample tilt with respect to the flat punch surface and results in incorrect elastic modulus values.
• Automated indentation results in incorrect values of the elastic modulus due to initial incomplete contact between the flat punch and the PDMS sample surface, caused by the tilt, and using the unloading slope, which is affected by viscoelastic soft polymer deformation.
• Correct procedure requires establishing the full contact between the tip and the sample. This is achieved by moving the tip into the sample in 1–2 μm increments, up to 40–80 μm maximum combined displacement, until the loading stiffness no longer increases.
• The elastic modulus is calculated from the loading stiffness and the diameter of the flat punch, instead of the unloading stiffness, which is larger due to viscoelastic unloading. After establishing the full contact, other mechanical testing can be conducted.

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