کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
231032 1427416 2012 7 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Supercritical fluid extraction of Alnus glutinosa (L.) Gaertn.
موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی مهندسی شیمی (عمومی)
پیش نمایش صفحه اول مقاله
Supercritical fluid extraction of Alnus glutinosa (L.) Gaertn.
چکیده انگلیسی

Supercritical carbon dioxide extraction of Alnus glutinosa (L.) Gaertn. was performed (P = 300/450 bar, T = 40/60 °C, EtOH addition = 0/5/10%) in order to determine preferable process conditions. Phytochemical composition of extracts were analyzed by means of TLC, GC–MS, LC–MS, RP-HPLC. Total of 11 pentacyclic triterpenes and β-sitosterol were identified. The results indicated that SFE is an advantageous method over Soxhlet extraction in terms of yield and recovery of target compounds. Overall extraction curves revealed that pressure had little influence on extraction yield, while temperature and amount of co-solvent increased it. The optimum SFE condition was 300 bar/60 °C/10% EtOH, where the amount of extracts was 3.81% compared to n-hexane (2.56%). Highest amount of betulin, betulinic acid and lupeol was 3.57, 2.95 and 14.33 g/100 g extract, respectively, depending on the applied SFE condition. Ethanolic Soxhlet extraction ensures the highest yield (40.90%), but provides the extracts diluted with undesirable substances hence the concentration of triterpenes in the extract was very low.

Figure optionsDownload as PowerPoint slideHighlights
► Supercritical fluid extraction of Alnus glutinosa (L.) Gaertn. was performed.
► Yields and pentacyclic triterpene composition of different extracts were evaluated.
► Pressure had little influence on the yield, while temperature and amount of co-solvent increased it.
► Presence of different triterpenoids and β-sitosterol were justified.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: The Journal of Supercritical Fluids - Volume 61, January 2012, Pages 55–61
نویسندگان
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