کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
53462 46971 2015 9 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Hydrothermal fractionation of grape seeds in subcritical water to produce oil extract, sugars and lignin
ترجمه فارسی عنوان
تجزیه هیدروترمال دانه های انگور در آب زیر کشت برای تولید عصاره روغن، قندها و لیگنین
موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی کاتالیزور
چکیده انگلیسی


• Grape seeds as a model compound for hydrothermal treatment and extraction.
• Multi-step temperature hydrolysis from 150 to 340 °C feasible for biomass fractionation.
• High lignin purity in the residual solid >90%.
• Extraction of 50–62% of sugars (0.20–0.23 g/g-grape).

In this work, the fractionation of grape seeds as a model biomass was studied using a combination of two processes: solvothermal extraction and hydrothermal fractionation-hydrolysis process in a semicontinuous reactor. First, grape seeds were subjected to an extraction process with ethanol/water (70/30 wt.%) at 90 °C during 60 min obtaining ca. 13.0 wt.% of oil and extractable components with 4.46 wt.% of polyphenols (66% of the maximum). Afterwards, the solvent was water and the biomass was treated in steps at different temperatures (150 °C to 340 °C). During the hydrolysis the pH decreased from 5.5 down to 3.0 due to acetyl group liberation. The total quantity of recovered sugars varied around 20.0 to 23.1 wt.%. The best experimental condition for obtaining the maximum amount of pentoses + hexoses + oligosaccharides was 180 °C (45 min) + 250 to 265 °C (45 min) + 330 to 340 °C (45 min).

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ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Catalysis Today - Volume 257, Part 2, 15 November 2015, Pages 160–168
نویسندگان
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