کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5448520 | 1511777 | 2017 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Amendment of saturation magnetization, blocking temperature and particle size homogeneity in Mn-ferrite nanoparticles using Co-Zn substitution
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
مواد الکترونیکی، نوری و مغناطیسی
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Nanocrystalline particles of compositions (CoZn)xMn1âxFe2O4 were prepared by the coprecipitation method from stoichiometric aqueous solutions, where x varies from 0 to 0.3 in steps of 0.05. The synthesized powders were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM) and Fourier transform infrared spectroscopy (FT-IR). A vibrating sample magnetometer (VSM) was used to measure the hysteresis parameters at 300 and 6Â K. Zero field cooling (ZFC) and field cooling (FC) curves were obtained at the temperature range 6-400Â K and the blocking temperature values were determined. XRD analysis confirmed the formation of the obtained powder in a single cubic spinel phase and it showed also that the lattice parameter is decreasing with the increase of (Co-Zn) content. FT-IR measurements between 160 and 650Â cmâ1 also confirmed the intrinsic cation vibrations of the spinel structure. The magnetic measurements showed that the saturation magnetization, coercivity and the values of blocking temperatures were increased with the (Co-Zn) content. TEM micrographs declared the improvement of particle size homogeneity with the increase of (Co-Zn) content without remarkable change in the average particle size. The obtained results were discussed in view of A-B sublattices interaction and superparamagnetic phenomenon.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Chemistry and Physics - Volume 186, 15 January 2017, Pages 505-512
Journal: Materials Chemistry and Physics - Volume 186, 15 January 2017, Pages 505-512
نویسندگان
M.M. Eltabey, A.M. Massoud, Cosmin Radu,