کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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58956 | 1419429 | 2015 | 6 صفحه PDF | دانلود رایگان |
The one-pot three-component cyclocondensation has been developed involving the reaction of benzil with an aromatic aldehydes and ammonium acetate under thermal solvent-free conditions in the presence of a KSF supported 10-molybdo-2-vanadophosphoric acid catalyst. 10-Molybdo-2- vanadophosphoric acid was immobilized on KSF with a 20% loading, which showed the highest catalytic activity. The catalyst was fully characterized using FT-IR spectroscopy, thermal analysis, XRD and SEM analysis techniques. There are several distinct advantages to this protocol, including high yields, short reaction time, operational simplicity and a recyclable catalyst with a facile work-up procedure.
Graphical AbstractTwenty percent 10-molybdo-2-vanadophosphoric acid supported on KSF clay acts as an efficient, green and reusable solid acid catalyst for one-pot synthesis of 2,4,5-trisubstituted imidazole derivatives.Figure optionsDownload as PowerPoint slide
Journal: Chinese Journal of Catalysis - Volume 36, Issue 7, July 2015, Pages 1054–1059