کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7598446 | 1492138 | 2014 | 9 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
A multi-residue method for the determination of pesticides in tea using multi-walled carbon nanotubes as a dispersive solid phase extraction absorbent
ترجمه فارسی عنوان
روش چند بقایی برای تعیین آفت کش ها در چای با استفاده از نانولوله های کربنی چند جداره به عنوان یک ماده جاذب جذب کننده فاز جامد
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
چکیده انگلیسی
A modified QuEChERS (quick, easy, cheap, effective, rugged and safe) method using multi-walled carbon nanotubes (MWCNTs) as a dispersive solid phase extraction (d-SPE) absorbent was established for analysis of 78 pesticide residues in tea. A 6 mg MWCNT sample was selected as the optimised amount based on the distribution of pesticide recoveries and clean-up efficiency from 6 mL acetonitrile extracts. The matrix effects of the method were evaluated and matrix-matched calibration was recommended. The method was validated employing gas chromatography coupled to tandem mass spectrometry (GC-MS/MS) at the spiked concentration levels of 0.05, 0.1 and 0.15 mg kgâ1. For most of the targeted pesticides, the percent recoveries range from 70% to 120%, with relative standard deviations (RSDs) <20%. The linear correlation coefficients (r2) were higher than 0.99 at concentration levels of 0.025-0.500 mg kgâ1. In this study, MWCNTs were proved to be a promising d-SPE absorbent with excellent cleanup efficiency, which could be widely applied for the analysis of pesticide residues.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Chemistry - Volume 153, 15 June 2014, Pages 121-129
Journal: Food Chemistry - Volume 153, 15 June 2014, Pages 121-129
نویسندگان
Xue Hou, ShaoRong Lei, ShiTing Qiu, LingAn Guo, ShengGuo Yi, Wei Liu,