کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7886038 | 1509784 | 2018 | 31 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Experimental planning of the synthesis of strontium molybdate by EDTA-citrate and its structural influence, morphology and optical bandgap
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Experimental planning of the synthesis of strontium molybdate by EDTA-citrate and its structural influence, morphology and optical bandgap Experimental planning of the synthesis of strontium molybdate by EDTA-citrate and its structural influence, morphology and optical bandgap](/preview/png/7886038.png)
چکیده انگلیسی
It was initially used a 23 experimental design with central point in triplicate to synthesize strontium molybdate by EDTA-citrate combined complexation method, where the influence of pH (6, 7.5 e 9), calcining time (3, 4 e 5â¯h) and heating rate (5, 7 e 10â¯Â°Câ¯minâ1) was investigated. Single-phase powders were obtained when calcined at 650â¯Â°C with tetragonal crystalline structure. The heating rate is the most influent independent variable on the intensities of the X-ray diffractions peaks. The synthesized powders are shown as agglomerates with irregular spherical and bipyramidal morphology. According to the experimental design, the conditions of calcining time of 3â¯h and heating rate of 10â¯Â°Câ¯minâ1 show the lowest values of energy band gap (4.18 and 4.17â¯eV) for pH 6 and 9, respectively. The statistical models generated were able to describe the phenomena observed.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 44, Issue 14, 1 October 2018, Pages 16606-16614
Journal: Ceramics International - Volume 44, Issue 14, 1 October 2018, Pages 16606-16614
نویسندگان
M.M.S. Silva, M.S. Sena, A.L. Lopes-Moriyama, C.P. Souza, A.G. Santos,