کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7886714 | 1509787 | 2018 | 28 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Influence of solid loading on the rheological, porosity distribution, optical and the microstructural properties of YAG transparent ceramic
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Stable aqueous dispersed mixture of commercial Al2O3 and Y2O3 nano powders was prepared by ball mill. Ammonium poly meta acrylate (Dolapix CE64) and tetraethyl orthosilicate (TEOS) were added as dispersant and sintering aid, respectively. The effects of slurry solid loading on the fabrication of transparent polycrystalline YAG ceramics by slip casting method were investigated. The rheological properties of slurries with different solid loading (64, 70 and 76â¯wt%) were studied by measuring the viscosity and shear stress as a function of shear rate. The effect of solid loadings on the porosity distribution was examined. The specimens were vacuum-sintered at 1715â¯Â°C for 10â¯h. Slips with 64 and 70â¯wt% solid loading behaved as near-Newtonian and as non-Newtonian with thixotropic behavior at 76â¯wt% solid loading. The relative densities of the green bodies increased from 58.0â¯Â±â¯0.6% (SDâ¯=â¯0.424) to 64.0â¯Â±â¯0.3% (SDâ¯=â¯0.228) by increasing the solid loading from 64â¯wt% to 70â¯wt% and then decreased to 63.0â¯Â±â¯0.2% (SDâ¯=â¯0.141) at 76â¯wt% solid loading. The results showed that the suitable solid loading for fabricating transparent YAG ceramics is 70â¯wt%. This sample had the narrowest pore size distribution (4-100â¯nm), homogenized surface fracture of green body, dense microstructure (99.990â¯Â±â¯0.005% final relative density, SDâ¯=â¯0.003) and the average grain size of 6â¯Âµm. It had the highest in-line transmittance, which was approximately 77% at 1064â¯nm.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 44, Issue 11, 1 August 2018, Pages 12098-12105
Journal: Ceramics International - Volume 44, Issue 11, 1 August 2018, Pages 12098-12105
نویسندگان
Fatemeh Mohammadi, Omid Mirzaee, Mohammad Tajally,