کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
7970484 1514387 2015 7 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Imaging and characterization of γ′ and γ″ nanoparticles in Inconel 718 by EDX elemental mapping and FIB-SEM tomography
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد دانش مواد (عمومی)
پیش نمایش صفحه اول مقاله
Imaging and characterization of γ′ and γ″ nanoparticles in Inconel 718 by EDX elemental mapping and FIB-SEM tomography
چکیده انگلیسی
Microstructural characterization of Inconel 718 superalloy after three different heat treatment variants was performed by electron microscopy and electron tomography techniques, taking advantage of recent development in quantitative electron microscopy. Distribution maps of the chemical elements, collected by ChemiSTEM™ EDX system, offer a clear contrast between γ′, γ″, and the γ matrix. It was found that the γ′ phase contains mainly Ni, Al, and Ti, while the γ″ phase contains Ni, Nb, and Ti. Thus application of the Al and Nb STEM-EDX elemental maps enables identification and size measurements of γ′ and γ″ nanoparticles. 3D morphology of γ′ and γ″ precipitates was examined by electron microscopy and FIB-SEM tomography. Employed methods revealed that in all three heat treatment variants the γ′ particles are almost spheroidal while the γ″ precipitates are mainly elongated-disc shaped. However, the precipitate sizes differed for each variant contributing to differences in the yield strength. Tomographic images were used for estimation of the volume fraction of the both strengthening phases.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Characterization - Volume 100, February 2015, Pages 74-80
نویسندگان
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