Analysis of peptides and proteins using sub-2 μm fully porous and sub 3-μm shell particles
Keywords: Fused-core; Core–shell; UHPLC; UPLC; Peptides; Proteins
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Oxidized and nitrated oleic acid in biological systems: Analysis by GC-MS/MS and LC-MS/MS, and biological significance
Keywords: BSTFA; N,O-bis(trimethylsilyl)trifluoroacetamide; CID; collision-induced dissociation; DIPEA; N,N-diisopropylethylamine; ECNICI; electron capture negative-ion chemical ionization; EI; electron ionization; cis-EpOA; cis-9,10-epoxyoctadecanoic acid; ESI; el
Multi-residue analysis of drugs of abuse in wastewater and surface water by solid-phase extraction and liquid chromatography–positive electrospray ionisation tandem mass spectrometry
Keywords: Illicit drugs; Drugs of abuse; Precursors; UPLC; Wastewater; Surface water; Environment; LC–MS/MS; Sewage; Crack cocaine; SPE; Pharmaceuticals; Multi-residue
Formation of 4-hydroxynonenal from cardiolipin oxidation: Intramolecular peroxyl radical addition and decomposition
Keywords: ALDH; aldehyde dehydrogenase; C-0; a water-soluble azo initiator; CID; collision-induced dissociation; CL; cardiolipin; DLPC; 1,2-dilinoleoyl-sn-glycero-3-phosphocholine; DNPH; 2,6-dinitrophenylhydrazine; ESI; electrospray ionization; 4-HNE; 4-hydroxy-2-n
Pollen metabolome analysis reveals adenosine as a major regulator of dendritic cell-primed TH cell responses
Keywords: Dendritic cells; immunomodulation; adenosine; pollen; allergy; ADA; Adenosine deaminase; APE; Aqueous pollen extract; cAMP; 3â²-5â²-Cyclic adenosine monophosphate; CFSE; Carboxyfluorescein succinimidyl ester; DC; Dendritic cell; FITC; Fluorescein isothi
Review of the applications of different analytical techniques for coxibs research
Keywords: ACN; acetonitrile; AI; active ingredient; APCI; atmospheric pressure chemical ionization; BCG; bromocresol green; BCP; bromocresol purple; CD; cyclodextrin; CE; capillary electrophoresis; CMS; chlorophenylmethylsulfone; COX; cyclooxygenase; CZE; capillary
Interferon-α 2b quantification in inclusion bodies using Reversed Phase-Ultra Performance Liquid Chromatography (RP-UPLC)
Keywords: Interferon-α 2b; UPLC; Validation; Inclusion body
Rapid product analysis and increased sensitivity for quantitative determinations of botulinum neurotoxin proteolytic activity
Keywords: HPLC; UPLC; Botulinum neurotoxin; Protease; Product analysis;
Simultaneous evaluation of intact glucosinolates and phenolic compounds by UPLC-DAD-MS/MS in Brassica oleracea L. var. botrytis
Keywords: UPLC; Tandem mass spectrometry; Flavonoids; Glucosinolates; Brassica oleracea; Sinapic acid
Clinical Pharmacokinetics of Paclitaxel Liposome with a New Route of Administration in Human Based on the Analysis with Ultra Performance Liquid Chromatography
Keywords: paclitaxel; liposome; intrapleural infusion; pleural fluid; plasma; clinical pharmacokinetics; UPLC;
Stability-indicating UPLC method for determination of Valsartan and their degradation products in active pharmaceutical ingredient and pharmaceutical dosage forms
Keywords: UPLC; Valsartan; Forced degradation; Validation; Stability-indicating
A validated stability-indicating UPLC method for desloratadine and its impurities in pharmaceutical dosage forms
Keywords: Development; Validation; Stability-indicating; UPLC; Desloratadine; Impurities
Comparison of positive and negative ion detection of tea catechins using tandem mass spectrometry and ultra high performance liquid chromatography
Keywords: UHPLC; Mass spectrometry; Tea; Phenolics; Catechins; Flavonoids; UPLC
UPLC/MS based method for quantitative determination of fatty acid composition in Gram-negative and Gram-positive bacteria
Keywords: APCI; Atmospheric pressure chemical ionization; APE; Absolute percent error; CFA; Cyclopropane fatty acids; EI; Electron ionization; ESI-MS; Electrospray ionization mass spectrometry; FAME; Fatty acid methyl esters; FFA; Free fatty acids; HPLC; High perfo
Comparative study of UPLC–MS/MS and HPLC–MS/MS to determine procyanidins and alkaloids in cocoa samples
Keywords: Alkaloids; Procyanidins; Phenols; Cocoa; HPLC; UPLC; MS/MS; Trace elements; Food analysis; Food composition
High throughput qualitative analysis of polyphenols in tea samples by ultra-high pressure liquid chromatography coupled to UV and mass spectrometry detectors
Keywords: Polyphenols; Catechins; Tea extract; LLE; UPLC; UHPLC; UPLC–MS/MS
Identification of a β-glucosidase hydrolyzing tuberonic acid glucoside in rice (Oryza sativa L.)
Keywords: JA; jasmonic acid; TA; tuberonic acid; TAG; tuberonic acid glucoside; MS/MS; tandem mass spectrometry; UPLC; ultra-performance liquid chromatography; MRM; multiple reaction monitoring; pNPG; p-nitrophyenyl β-glucoside; Oryza sativa L. cv. Kitaake; Gramin
A high throughput metabolic stability screening workflow with automated assessment of data quality in pharmaceutical industry
Keywords: Intelligent; Workflow; High throughput; Metabolic stability assay; Microsomal stability assay; Sample pooling; Cassette analysis; UPLC; UHPLC; MS; Mass spectrometry; Automation
Characterization of steroidal saponins in crude extracts from Dioscorea zingiberensis C. H. Wright by ultra-performance liquid chromatography/electrospray ionization quadrupole time-of-flight tandem mass spectrometry
Keywords: Steroidal saponin; Dioscorea zingiberensis C. H. Wright; UPLC; Q-TOF-MS/MS; Structural elucidation
A novel rapid method for simultaneous determination of eight active compounds in silymarin using a reversed-phase UPLC-UV detector
Keywords: UPLC; HPLC; Silymarin; Gradient analysis
Validated UPLC method for the fast and sensitive determination of steroid residues in support of cleaning validation in formulation area
Keywords: Steroid separation; UPLC; Method validation; Cleaning validation; High speed separation;
Determination of biogenic amines in foods using ultra-performance liquid chromatography (UPLC)
Keywords: UPLC; HPLC; Biogenic amines; Determination; Foods; Putrescine; Histamine
Rapid and quantitative screening method for 43 benzodiazepines and their metabolites, zolpidem and zopiclone in human plasma by liquid chromatography/mass spectrometry with a small particle column
Keywords: LC/MS; UPLC; Benzodiazepines; Focus™; Drug screening
Development of a sensitive and selective LC-MS/MS method for simultaneous determination of gemcitabine and 2,2-difluoro-2-deoxyuridine in human plasma
Keywords: Gemcitabine; 2,2-Difluoro-2-deoxyuridine; Derivatization; Dansyl chloride; Mass spectrometry; UPLC;
Screening for metabolites of acarviostatin family aminooligosaccharides in rats using ultraperformance liquid chromatography coupled with electrospray ionization tandem mass spectrometry
Keywords: Acarviostatin II03; Acarviostatin III03; Metabolites; UPLC; MS
UPLC/Q-TOFMS/MS as a powerful technique for rapid identification of polymethoxylated flavones in Fructus aurantii
Keywords: UPLC; Q-TOFMS/MS; PMFs; Fructus aurantii; Rapid identification; Mass spectrometric fingerprint
Automated method for the direct analysis of 8-oxo-guanosine and 8-oxo-2′-deoxyguanosine in human urine using ultraperformance liquid chromatography and tandem mass spectrometry
Keywords: 8-oxodG, 8-oxo-2′-deoxyguanosine; 8-oxoGuo, 8-oxo-guanosine; ISTD, internal standardOxidative stress; 8-oxodG; 8-oxoGuo; Human urine; UPLC; Mass spectrometry
Metabolomics: A New Frontier for Research in Pediatrics
Keywords: CSF; Cerebrospinal fluid; HPLC; High-performance liquid chromatography; IBD; Inflammatory bowel disease; LC-MS; Liquid chromatography-mass spectrometry; MS; Mass spectrometry; MSI; Metabolomics standard initiative; NMR; Nuclear magnetic resonance; UPLC;
A confirmatory method for the simultaneous extraction, separation, identification and quantification of Tetracycline, Sulphonamide, Trimethoprim and Dapsone residues in muscle by ultra-high-performance liquid chromatography–tandem mass spectrometry accord
Keywords: Antibiotics; Multi-residue; UPLC; Method validation; Tetracyclines; Sulphonamides; Trimethoprim; Dapsone; Mass spectrometry; Muscle
Fast determination of 26 amino acids and their content changes in royal jelly during storage using ultra-performance liquid chromatography
Keywords: UPLC; Free amino acid; Total amino acid; Royal jelly; Storage condition; Food composition
Determination of procyanidins and their metabolites in plasma samples by improved liquid chromatography–tandem mass spectrometry
Keywords: Plasma; Procyanidins; Tandem mass spectrometry; UPLC
Simultaneous extraction and screening of diuretics, beta-blockers, selected stimulants and steroids in human urine by HPLC-MS/MS and UPLC-MS/MS
Keywords: UPLC; Tandem mass spectrometry; Diuretics; Beta-blockers; Stimulants; Urine; Doping
Simultaneous quantitative analysis of N-acylethanolamides in clinical samples
Keywords: N-acylethanolamides; AEA; OEA; PEA; Virodhamine; Clinical samples; UPLC; MS
Metabolite profiling of plant extracts by ultra-high-pressure liquid chromatography at elevated temperature coupled to time-of-flight mass spectrometry
Keywords: UPLC; HTLC; UHPLC; HT-UPLC; Temperature; Degradation; Profiling; Plant extract; Peak capacity
Ultra-performance liquid chromatography-tandem mass spectrometry for rapid and highly sensitive analysis of stereoisomers of benzo[a]pyrene diol epoxide-DNA adducts
Keywords: UPLC; ESI-MS/MS; Benzo[a]pyrene; DNA adducts;
Isolation of two Pseudomonas strains producing pseudomonic acid A
Keywords: Mupirocin; Pseudomonas fluorescens; Environmental isolates; FT-ICR-MS; UPLC; HPLC; Antibiotic
Effects of extra-column band spreading, liquid chromatography system operating pressure, and column temperature on the performance of sub-2-μm porous particles
Keywords: Band spreading; UPLC; Kinetic plots; Sub-2-μm particles
Purification, characterization, and cDNA cloning of acidic platelet aggregation inhibiting phospholipases A2 from the snake venom of Vipera lebetina (Levantine viper)
Keywords: Snake venom; Vipera lebetina; Phospholipase A2; cDNA cloning; Platelet aggregation inhibition; VLPLA2; Vipera lebetina phospholipase A2; TFA; trifluoroacetic acid; p-BPB; p-bromophenacylbromide; MALDI-TOF MS; matrix assisted laser desorption ionization ti
Ultra high performance liquid chromatography tandem mass spectrometric detection in clinical analysis of simvastatin and atorvastatin
Keywords: Atorvastatin; Simvastatin; Hemodialysis; UPLC; Tandem mass spectrometry; Bio-analytical method;
Coupling ultra high-pressure liquid chromatography with single quadrupole mass spectrometry for the analysis of a complex drug mixture
Keywords: Fast-LC; Pharmaceutical; UHPLC; UPLC; UHPLC–MS
Comparison of electrospray ionization, atmospheric pressure chemical ionization and atmospheric pressure photoionization for determining estrogenic chemicals in water by liquid chromatography tandem mass spectrometry with chemical derivatizations
Keywords: Dansyl chloride; Matrix effect; Pentafluorobenzyl bromide; UPLC; Steroid estrogen; 2D-LC
Drugs of abuse testing by tandem mass spectrometry: A rapid, simple method to replace immunoassays
Keywords: Drugs of abuse; Tandem mass spectrometry; Toxicology; UPLC; Chromatography; GC/MS; Screening
Some solutions to obtain very efficient separations in isocratic and gradient modes using small particles size and ultra-high pressure
Keywords: UPLC; UHPLC; HTLC; Temperature; Gradient; Peak capacity; Very high resolution
Determination of opiates and cocaine in urine by high pH mobile phase reversed phase UPLC–MS/MS
Keywords: UPLC; LC–MS/MS; Opiates; Opioids; Cocaine; High pH mobile phase; Reversed phase; Forensic toxicology
Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry
Keywords: Milk; Veterinary drugs; Fast liquid chromatography; UPLC; Time of flight; Mass spectrometry
Herbal medicine analysis by liquid chromatography/time-of-flight mass spectrometry
Keywords: Liquid chromatography; RRLC; UPLC; Time-of-flight mass spectrometry; Chemical analysis; Herbal medicines; Medicinal plants; Chinese herbal medicines; Traditional Chinese medicines
Comparative accumulation and composition of lipophilic marine biotoxins in passive samplers and in mussels (M. edulis) on the West Coast of Ireland
Keywords: AZA; Marine toxins; OA; Passive sampling; PTX; SPATT; SPX; UPLC; YTX
Methods for the analysis of oxylipins in plants
Keywords: ALA; α-linolenic acid; AOC; allene oxide cyclase; AOS; allene oxide synthase; CI; chemical ionization; CID; collisionally induced dissociation; DAD; diode array detection; DES; divinyl ether synthase; DGDG; digalactosyl diacylglycerol; DGMG; digalactosyl
Rapid determination of aflatoxins in corn and peanuts
Keywords: Aflatoxins; Corn; Peanut; UPLC