کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10385129 | 882533 | 2014 | 9 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Flow and mixing efficiency characterisation in a CO2-assisted single-screw extrusion process by residence time distribution using Raman spectroscopy
ترجمه فارسی عنوان
خصوصیات جریان و مخلوط سازی کارایی در یک فرآیند اکستروژن تک پیچ توسط توزیع زمان اقامت با استفاده از طیف سنجی رامان
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کلمات کلیدی
اکستروژن داغ ذوب، دی اکسید کربن فوق بحرانی، توزیع زمان اقامت، میکسر استاتیک، طیف سنجی رامان،
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی شیمی
تصفیه و جداسازی
چکیده انگلیسی
Hot-melt extrusion of a bio-sourced polyamide has been implemented in a single-screw extruder with supercritical carbon dioxide injection. CO2 acts as a plasticiser in the extruder barrel and as a physical blowing agent at the die. To insure a better mixing and dissolution of the CO2 into the polymer melt, addition of a static mixer between the screw tip and the die was tested. The effect of both the static mixing element and the CO2 injection on the melt flow behaviour has been elucidated. A recent technique of in-line Raman spectroscopy was implemented to make a residence time distribution study, using titanium dioxide as a tracer. The use of a static mixer exerts a major modification on the flow behaviour: it improves mixing by enhancing dispersion. In addition, the structure of the manufactured products was studied: the static mixer led to more homogeneous porous structure. The broad range of CO2 incorporation (up to 25%, w/w) into the melt led to the manufacture of foams with adjustable porosity from 15 to 70%.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Chemical Engineering Research and Design - Volume 92, Issue 7, July 2014, Pages 1210-1218
Journal: Chemical Engineering Research and Design - Volume 92, Issue 7, July 2014, Pages 1210-1218
نویسندگان
Audrey Common, Elisabeth Rodier, Martial Sauceau, Jacques Fages,