کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10540955 | 963417 | 2012 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Optimisation and validation of a specific analytical method for the determination of thiram residues in fruits and vegetables by LC-MS/MS
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Optimisation and validation of a specific analytical method for the determination of thiram residues in fruits and vegetables by LC-MS/MS Optimisation and validation of a specific analytical method for the determination of thiram residues in fruits and vegetables by LC-MS/MS](/preview/png/10540955.png)
چکیده انگلیسی
⺠Specific analytical methodology is developed for determination of dithiocarbamate fungicide thiram in fruits and vegetables. ⺠The method is based on LC coupled to tandem MS. ⺠Thiram degradation along sample treatment is minimised, adding specific reagents and operating at around 5 °C. ⺠The excellent sensitivity and selectivity of the method allows monitoring for compliance of MRLs, with LOQ of 0.01 mg/kg. ⺠The acquisition of several SRM transitions allows the reliable confirmation of thiram in the samples at very low levels.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Chemistry - Volume 135, Issue 1, 1 November 2012, Pages 186-192
Journal: Food Chemistry - Volume 135, Issue 1, 1 November 2012, Pages 186-192
نویسندگان
Aranzazu Peruga, Susana Grimalt, Francisco J. López, Juan V. Sancho, Félix Hernández,