کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1215870 | 966985 | 2007 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Microemulsion electrokinetic chromatography for the separation of arctiin and arctigenin in Fructus Arctii and its herbal preparations
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
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چکیده انگلیسی
A microemulsion electrokinetic chromatography method was used to separate arctiin and arctigenin in Fructus Arctii and its herbal preparations. The separation of arctiin and arctigenin was performed using a 1-butanol–SDS–ethyl acetate–water microemulsion in 10 mM sodium tetraborate buffer. The analytes were baseline-resolved within 4 min. In the concentration range 5–500 μg/mL, the calibration curves reveal linear relationships between the peak area for each analyte and its concentration (correlation coefficients: 0.9993 for arctiin and 0.9998 for arctigenin). The method was applied to the analysis of arctiin and arctigenin in herbal preparations, and the recoveries were 98.7–103.1% for arctiin and 97.6–103.2% for arctigenin, respectively.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Chromatography B - Volume 860, Issue 1, 1 December 2007, Pages 127–133
Journal: Journal of Chromatography B - Volume 860, Issue 1, 1 December 2007, Pages 127–133
نویسندگان
Wenjuan Lü, Yonglei Chen, Yuxia Zhang, Xiuping Ding, Hongli Chen, Mancang Liu,