کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1236864 968878 2009 7 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Synthesis and characterization of a new organic nonlinear optical crystal: l-Phenylalaninium maleate
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
Synthesis and characterization of a new organic nonlinear optical crystal: l-Phenylalaninium maleate
چکیده انگلیسی
l-Phenylalaninium maleate (abbreviated as LPM) chemical formula C9H12NO2+·C4H3O4−, a new organic nonlinear optical crystal was grown by slow evaporation technique. Transparent needle shaped crystal of dimensions 7 mm × 1 mm × 0.5 mm was obtained. Single crystals of LPM have been subjected to X-ray diffraction analysis to estimate the lattice parameters and the space group. The powder X-ray diffractogram of the crystal has been recorded and the reflections from various planes are identified. The XRD studies confirm the crystalline nature. The qualitative analysis on the crystal has been carried out using Fourier transform infrared (FTIR) and Fourier transform Raman (FTRaman) spectral measurements. The presence of hydrogen and carbon in the grown crystal was confirmed by using proton and carbon nuclear magnetic resonance (NMR) spectral analyses. Optical behaviour of the crystal was investigated using UV-vis spectroscopy. The thermal stability of the crystal was analysed with the aid of thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). The nonlinear optical (NLO) property of the crystal was tested by Nd:YAG laser source.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy - Volume 74, Issue 4, November 2009, Pages 917-923
نویسندگان
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