کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1390212 | 1500865 | 2014 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis of bis-cellobiose and bis-glucose derivatives of azacrown macrocycles as hosts in complexes with acetylsalicylic acid and 4-acetamidophenol
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Synthesis of bis-cellobiose and bis-glucose derivatives of azacrown macrocycles as hosts in complexes with acetylsalicylic acid and 4-acetamidophenol Synthesis of bis-cellobiose and bis-glucose derivatives of azacrown macrocycles as hosts in complexes with acetylsalicylic acid and 4-acetamidophenol](/preview/png/1390212.png)
چکیده انگلیسی
• Tandem Staudinger/aza-Wittig reaction of a 1-azidosaccharide derivatives with azacrown ethers.
• Complexing properties received macrocycles towards to acetylsalicylic acid and 4-acetamidophenol.
• Stoichiometry of complexes indicated by the Job’s plot using 1H NMR spectroscopy.
Two new C2 symmetric bis-cellobiose and bis-glucose azacrown derivatives were prepared according to the one-step procedure using azacrown ethers and azidosaccharides. Their complexes with aspirin and paracetamol were studied with the use of proton NMR spectroscopy. It was found that these pseudocryptands bind aspirin and paracetamol but each one in a different manner.
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ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Research - Volume 386, 11 March 2014, Pages 18–22
Journal: Carbohydrate Research - Volume 386, 11 March 2014, Pages 18–22
نویسندگان
Michalina Pintal, Bogusław Kryczka, Alain Marsura, Stanisław Porwański,