کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1483640 1510509 2009 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Hydrogen embrittlement assisted by ball-milling to obtain AlCuFe nanoparticles
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
Hydrogen embrittlement assisted by ball-milling to obtain AlCuFe nanoparticles
چکیده انگلیسی
In this work, we show that the synthesis of AlCuFe nanoparticles can be achieved by a wet ball-milling process. The AlCuFe intermetallic system is highly sensitive to the environmental embrittlement mechanism. Taking advantage of this, the wet ball-milling was used to increase the rate of grinding and accelerate the characteristic cleavage fracture of these phases. This research was carried out by subjecting Al64Cu24Fe12 pre-alloyed ribbons to high-energy ball-milling under different powder-humidity relationships. The pre-alloyed and milled powders were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), and scanning transmission electron microscopy (STEM). High resolution electron microscopy (HREM) measurements and energy-dispersive X-ray spectroscopy (EDXS) elemental chemical mapping confirm that the nanoparticles have a BCC structure with Al-Cu-Fe chemical composition. During the wet ball-milling, the aluminum content in the ψ-phase diminishes due to embrittlement mechanism which provokes its aperiodic disarrangement. This aluminum loss could be related with a ψ-β transformation.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Non-Crystalline Solids - Volume 355, Issues 34–36, 15 September 2009, Pages 1713-1718
نویسندگان
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