Analysis of the decomposition gases from α and β-Cd(BH4)2 synthesized by temperature controlled mechanical milling

► Temperature controlled metathesis reaction of LiBH4 with CdCl2. ► Temperature controlled mechanical synthesis of alpha and beta Cd(BH4)2. ► Semi-quantitative analysis of the decomposition gases, 1:1 H2 + B2H6, released by Cd(BH4)2.