کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1623443 | 1516406 | 2009 | 4 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Magnetic properties of nanostructured Fe92P8 powder mixture
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فلزات و آلیاژها
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Magnetic properties of nanostructured Fe92P8 powder mixture Magnetic properties of nanostructured Fe92P8 powder mixture](/preview/png/1623443.png)
چکیده انگلیسی
Structural and magnetic properties of nanostructured Fe92P8 (wt.%) powder mixture prepared by mechanical alloying were investigated by X-ray diffraction (XRD), Mössbauer spectrometry and magnetic measurements. The crystallite sizes were found to decrease with milling time to the nanometer scale (6-14 nm). Milling for 21 h gives rise to a mixture of: (i) a two-bcc α-Fe structure with the same lattice parameter but different microstructural (crystallite size, microstrain) and hyperfine parameters (magnetic field, isomer shift), (ii) Fe3P nanophase and (iii) a small amount of a paramagnetic FeP phosphide phase, not exceeding 2%. Furthermore, the temperature dependence of the magnetic susceptibility measurement reveals the presence of two magnetic phases with different Curie temperatures, Tc1 and Tc2. One Curie temperature is nearly constant (Tc1 = 867 K) during the milling process, while the other one (Tc2) is milling time dependent. Annealing at a temperature of 210 °C for half an hour leads to the formation of the FeP phosphide in addition to an α-Fe(P) solid solution and the Fe3P nanophase.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Alloys and Compounds - Volume 471, Issues 1â2, 5 March 2009, Pages 24-27
Journal: Journal of Alloys and Compounds - Volume 471, Issues 1â2, 5 March 2009, Pages 24-27
نویسندگان
R. Bensalem, W. Tebib, S. Alleg, J.J. Suñol, L. Bessais, J.M. Greneche,