کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1652308 1007640 2008 4 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Synthesis of α-alumina powder with internal nanostructures from Al13-cluster
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
Synthesis of α-alumina powder with internal nanostructures from Al13-cluster
چکیده انگلیسی

Nanostructured α-alumina powder was synthesized by precipitation and calcination of Al13-clusters that were formed by the hydrolysis of Al3+ions with hydroxide. The Al13-clusters were precipitated with oxalic acid by two-stage and one-stage precipitation techniques. The precipitates were calcined in air at 1100 °C. The resulting α-alumina particles were characterized using particle size analyzer, X-ray diffraction (XRD) and transmission electron microscope (TEM). The pH and precipitation technique were found to influence the microstructural features of the α-alumina powder produced. Alumina with more extensive nanostructures inside the grain can be produced through the two-stage precipitation technique.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Letters - Volume 62, Issue 15, 31 May 2008, Pages 2339–2342
نویسندگان
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