کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1678360 1009940 2008 10 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Characterization of JEOL 2100F Lorentz-TEM for low-magnification electron holography and magnetic imaging
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
Characterization of JEOL 2100F Lorentz-TEM for low-magnification electron holography and magnetic imaging
چکیده انگلیسی

We present results that characterize the performance and capabilities of the JEOL 2100F-LM electron microscope to carry out holography and quantitative magnetic imaging. We find the microscope is well-suited for studies of magnetic materials, or for semi-conductor dopant profiling, where a large hologram width (∼1 μm) and fine fringe spacing (∼1.5 nm) are obtained with good contrast (∼20%). We present, as well, measurements of the spherical aberration coefficient Cs=(108.7±9.6) mm and minimum achievable focal step δf=(87.6±1.4) nm for the specially designed long-focal-length objective lens of this microscope. Further, we detail experiments to accurately measure the optical parameters of the imaging system typical of conventional holography setup in a transmission electron microscope. The role played by astigmatic illumination in the hologram formation is also assessed with a wave-optical model, which we present and discuss. The measurements obtained for our microscope are used to simulate realistic holograms, which we compare directly to experimental holograms finding good agreement. These results indicate the usefulness of measuring these optical parameters to guide the optimization of the experimental setup for a given microscope, and to provide an additional degree of practical experimental possibility.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultramicroscopy - Volume 108, Issue 7, June 2008, Pages 625–634
نویسندگان
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