کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
234447 | 465411 | 2007 | 4 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Determination of ultra-trace selenium in mineral samples by hydride generation atomic fluorescence spectrometry with pressurized-PTFE-vessel acid digestion
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موضوعات مرتبط
مهندسی و علوم پایه
مهندسی شیمی
مهندسی شیمی (عمومی)
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چکیده انگلیسی
Pressurized polytetrafluoroethylene (PTFE) vessel acid digestion was applied in decomposition of sediments, soil and rock samples. Sensitive and accurate detection of selenium was achieved by hydride generation atomic fluorescence spectrometry (HG-AFS) with a low detection limit of 0.008 μg g−1. Aliquots (25 mg) of dried samples were decomposed with 0.5 mL HCl, and 0.5 mL HBF4 in closed pressurized PTFE vessels in an electronic oven at 125 °C for 5 h. Obtained and certified selenium concentrations for Chinese certified reference materials showed no statistically differences. Low detection limits and good repeatability made this method an accurate and useful tool for selenium analysis in sediments, soil and rock samples.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Minerals Engineering - Volume 20, Issue 15, December 2007, Pages 1397–1400
Journal: Minerals Engineering - Volume 20, Issue 15, December 2007, Pages 1397–1400
نویسندگان
Ni Zhang, Genling Sun, Hairui Ma,