کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5156930 | 1500593 | 2017 | 24 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Determination of carrageenan by means of photometric titration with Methylene Blue and Toluidine Blue dyes
ترجمه فارسی عنوان
تعیین کاراگینان با استفاده از تیتراسیون فوتومتریک با رنگ آمیزی متیلن آبی و تولویدین آبی
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کلمات کلیدی
کاراژین، پلی ساکارید آنیونی، متاکرومیا، تیتراسیون اتوماتیک،
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
چکیده انگلیسی
A new approach to carrageenan quantitation was described. The method consists in titration of carrageenan solution by Methylene Blue dye or Toluidine Blue dye solution until a certain absorbance value. The optimal wavelengths are 660Â nm and 640Â nm when titrating with Methylene Blue dye and Toluidine Blue dye, respectively. Rectilinear calibration plots (R2Â >Â 0.996) provide carrageenan determination in the concentration range from 2 to 60Â mg/L with relative standard deviation from 1 to 5%. The proposed method is simple and feasible in use due to optical dip probe providing in situ absorbance measurements. The proposed way of end-point recognition as pre-set voltage is applicable with any automatic titrator. The method was tested on model jelly dessert sachet. No interference was registered from typical ingredients of jellies such as sucrose, citric acid, sodium citrate, malic acid, potassium sorbate as well as blue colorant. The neutral polysaccharides such as guar gum and locust bean gum have insignificant interference when their content is fivefold as compared to that of carrageenan.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Polymers - Volume 165, 1 June 2017, Pages 1-6
Journal: Carbohydrate Polymers - Volume 165, 1 June 2017, Pages 1-6
نویسندگان
Dorota ZióÅkowska, Agnieszka Kaniewska, Jan Lamkiewicz, Alexander Shyichuk,