کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5206874 | 1382325 | 2011 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
On gel determination in PA6-glass fiber composites
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
پیش نمایش صفحه اول مقاله
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چکیده انگلیسی
Engineering plastics are frequently reinforced but the testing procedures are in many cases significantly affected by the presence of the reinforcing agent. A method for gel content determination in PA-6/glass fiber composite crosslinked by irradiation was investigated based on extraction of the sample fraction soluble in 90% formic acid. The sample, wrapped in glass fabric, was treated under ten selected modes to optimize the analysis. Shape of the analyzed sample was shown to be important. Applying statistical tests to the results, an optimal procedure was developed that consisted of sample extraction by the solvent under mild shaking for 24Â h and then removing the excessive solvent followed by drying the sample. A correction for the fraction of the glass fabric lubricant extractable by the solvent was necessary for calculation of correct results. A gel content of approximately 60Â wt.% was determined with relative standard deviation less than 5%.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Polymer Testing - Volume 30, Issue 5, August 2011, Pages 472-477
Journal: Polymer Testing - Volume 30, Issue 5, August 2011, Pages 472-477
نویسندگان
Mária Porubská, Danica Äervinková, Ivan Chodák,