کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
5407165 1393205 2008 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
3D 1H-13C-14N correlation solid-state NMR spectrum
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی تئوریک و عملی
پیش نمایش صفحه اول مقاله
3D 1H-13C-14N correlation solid-state NMR spectrum
چکیده انگلیسی
Nitrogen-14 (spin I = 1) has always been a nucleus difficult to observe in solid-state NMR and until recently its observation was restricted to one-dimensional (1D) spectra. We present here the first 3D 1H-13C-14N NMR correlation spectrum. This spectrum was acquired on a test sample l-histidine·HCl·H2O using a recently developed technique, which consists in indirectly observing 14N nuclei via dipolar recoupling with an HMQC-type experiment.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Magnetic Resonance - Volume 193, Issue 2, August 2008, Pages 321-325
نویسندگان
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