کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5469101 | 1519052 | 2017 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Rapid preparation of nano hexagonal-shaped hydrocalumite via one-pot mechanochemistry method
ترجمه فارسی عنوان
آماده سازی سریع هیدروالالومیت شکل نانو شش ضلعی با استفاده از روش مکانیکونی یک پشته
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
علوم زمین و سیارات
ژئوشیمی و پترولوژی
چکیده انگلیسی
Hexagonal-shaped hydrocalumite (Ca-Al layered double hydroxides) was successfully synthesized by one-step mechanochemistry method within only 30Â min. The product was characterized by X-ray diffraction, Fourier Transform Infrared spectroscopy, field emission scanning electron microscopy, energy dispersive spectroscopy, elemental mapping analysis, transmission electron microscopy, X-ray fluorescence, and thermogravimetric analysis. The results showed that the formation of a well-defined hydrocalumite and the microstructural evolution were strongly dependent on the milling time. From XRD profiles, a well-crystallized hydrocalumite with higher peaks intensity was formed after 60Â min of milling, while the sharpness and intensity of LDH-derived XRD peaks decreased as milling time increased. Microscopic analysis showed that the product had hexagonal layered structure with lateral dimension of 100 to 200Â nm. In addition, the thermal decomposition of the product is reported in details. This study offers a low-cost approach to synthesis of hydrocalumite owing to simplicity and extremely short processing time.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Applied Clay Science - Volume 136, February 2017, Pages 90-95
Journal: Applied Clay Science - Volume 136, February 2017, Pages 90-95
نویسندگان
Abbas Fahami, Gary W. Beall, Saeid Enayatpour, Fariborz Tavangarian, Mohammad Fahami,