کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
582531 | 1453164 | 2009 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
High performance liquid chromatography of 1,1-diamino-2,2-dinitroethene and some intermediate products of its synthesis
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موضوعات مرتبط
مهندسی و علوم پایه
مهندسی شیمی
بهداشت و امنیت شیمی
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چکیده انگلیسی
In the paper, the results of research the purity of DADNE in different recrystallization conditions and some intermediate products of its synthesis were presented. High performance liquid chromatography (HPLC) method based on the porous graphitic carbon (PGC) column packing material has been developed. Two variants of mobile phases in different pH values: acetonitrile-water and methanol-water with ammonia (NH3) and with trifluoroacetic acid (TFA) were used. The probable mechanism of interaction between the analyte, the stationary phase, and the mobile phase was suggested.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Hazardous Materials - Volume 164, Issues 2â3, 30 May 2009, Pages 1051-1058
Journal: Journal of Hazardous Materials - Volume 164, Issues 2â3, 30 May 2009, Pages 1051-1058
نویسندگان
BogusÅaw Buszewski, Monika Michel, StanisÅaw CudziÅo, Zbigniew ChyÅek,