Short CommunicationPilot survey of methamphetamine in sewers using a Polar Organic Chemical Integrative Sampler

- Polar Organic Chemical Integrative Samplers (POCIS) were deployed into sewer lines.
- Proof-of-concept was established for using POCIS devices in the sewage system.
- POCIS sorbent extracts were analyzed via HPLC-MS/MS.
- Methamphetamine was detected within the sewage collection system.
- The data encourage research for future use as a forensic tool in law enforcement.

A pilot study for the qualitative detection of methamphetamine at sites within a sewage collection system adjacent to locations suspected to harbor illegal drug activities was investigated and preliminary findings are reported. Sewage samples were collected over a time interval of four weeks using a Polar Organic Chemical Integrative Sampler (POCIS) deployed directly into the sewer line. The POCIS sorbent was extracted and analyzed via high-performance liquid chromatography tandem mass spectrometry (HPLC-MS/MS). Methamphetamine was found in sewage from one of three sampling sites at a concentration greater than the HPLC-MS/MS method detection limit (MDL) of 3 ng/mL. The goal of this research was to establish proof-of-concept of the feasibility for sampling and analysis using POCIS devices in the sewage collection system. The data encourage further testing and research. The ability to pinpoint the presence of methamphetamine in the sewer may in the future be used as a forensic tool in law enforcement.