Ultrasonic-assisted extraction and purification of phenolic compounds from sugarcane (Saccharum officinarum L.) rinds

- UAE technique was applied for the fast extraction of phenolic compounds.
- RSM was launched to investigate for the optimization of the UAE.
- MARs X-5 were most suitable for purification of phenolic compounds.
- Sugarcane rind is rich in gallic acid, chlorogenic acid and ferulic acid.

In order to obtained highest extraction efficiency of phenolic compounds from the sugarcane rinds, a rapid extraction method based on ultrasound-assisted extraction technique using response surface methodology was investigated. Results showed that the optimal conditions were: solvent concentration 52.19 mL/100 mL, solid-liquid ratio 14.46 mL/g, ultrasonic temperature 61.54 °C and extraction time 31.30 min. The practical phenolic compounds extraction rate was 8.67 g/100 g DW, which was well matched with the predicted value of 8.82 g/100 g DW. Purified by macroporous resins adsorption or solvent extraction method, the total phenolic content of crude phenolic compounds extracts improved from 117.50 ± 13.00 to 302.50 ± 19.50 or 670.00 ± 17.00 mg/g, respectively. Gallic acid, chlorogenic acid and ferulic acid were identified as three main phenolic compounds in the phenolic compounds extract by HPLC analysis. Furthermore, TPC revealed good correlations with antioxidant activities. All of the results indicated that sugarcane rinds could be used as a good source of phenolic compounds with significant antioxidant activities.