کد مقاله کد نشریه سال انتشار مقاله انگلیسی ترجمه فارسی نسخه تمام متن
690602 1460422 2015 7 صفحه PDF سفارش دهید دانلود رایگان
عنوان انگلیسی مقاله ISI
Preparation of vanadium-doped titanium dioxide neutral sol and its photocatalytic applications under UV light irradiation
ترجمه فارسی عنوان
آماده سازی زون خنثی دی اکسید تیتانیوم وانادیوم و کاربرد آن در فتوکاتالیتی تحت نور اشعه ماوراء بنفش
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موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی تکنولوژی و شیمی فرآیندی
چکیده انگلیسی
A sol-gel method was used to prepare V-doped TiO2 sol. TiCl4 was converted to Ti(OH)4 and H2O2 was then added to convert it to TiO2 at high temperature. The sols with various contents of V were used to prepared thin films on glass substrate by dip-coating method. The as-prepared samples were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope, high resolution transmission electron microscope (HRTEM), X-ray photoelectron spectroscopy, and UV-vis spectroscopy. The photocatalytic activities of the V-TiO2 thin films were investigated by the degradation of methylene blue under UV light irradiation. The as-prepared V-TiO2 sol was neutral and showed high stability of nanoparticles suspended in the sol without any surfactant. The shape of particle was rhombus and possessed high aspect ratio. The V-TiO2 particles were in anatase and nanosize, so they do not need annealing process to form crystals after coating on the substrate. V doping can produce more photogenerated electrons and holes, which improved the photocatalytic activity. However, overdoes V in TiO2 would lead to form the recombination centers and suppressed the activity. The optimum NH4VO3/TiO2 weight ratio in starting materials was 3%.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of the Taiwan Institute of Chemical Engineers - Volume 52, July 2015, Pages 140-146
نویسندگان
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