کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7886730 | 1509786 | 2018 | 21 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Maghemite, γ-Fe2O3, nanoparticles preparation via carbon-templated solution combustion synthesis
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
High surface area maghemite, γ-Fe2O3, nanoparticles were prepared via carbon-templated solution combustion synthesis, which is a two-step approach. Step one involves the combustion synthesis of maghemite nanoparticles embedded in an amorphous carbon matrix, by using a fuel rich reaction mixture of triethylenetetramine and iron nitrate. Step two consists of residual carbon removal by treating the previously-obtained composite precursor with hydrogen peroxide, which releases the maghemite nanopowder. This approach avoids carbon removal by thermal treatment, thus preserving the nanometric size of maghemite nanoparticles (8-12â¯nm), yielding a high specific surface area of 191.9â¯m2/g. At the same time, the final maghemite nanoparticles presented a superparamagnetic behavior and a saturation magnetization of 26.2â¯emu/g, in relation to the small particle size.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 44, Issue 12, 15 August 2018, Pages 14090-14094
Journal: Ceramics International - Volume 44, Issue 12, 15 August 2018, Pages 14090-14094
نویسندگان
Robert IanoÈ, Elena-Alina MoacÄ, Aylin CÄpraru, Radu LazÄu, Cornelia PÄcurariu,