کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
8038098 1518323 2015 12 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
The effect of pattern overlap on the accuracy of high resolution electron backscatter diffraction measurements
ترجمه فارسی عنوان
اثر الگوی همپوشانی بر روی دقت اندازه گیری پراکندگی الکترون برگشتی با وضوح بالا
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
چکیده انگلیسی
High resolution, cross-correlation-based, electron backscatter diffraction (EBSD) measures the variation of elastic strains and lattice rotations from a reference state. Regions near grain boundaries are often of interest but overlap of patterns from the two grains could reduce accuracy of the cross-correlation analysis. To explore this concern, patterns from the interior of two grains have been mixed to simulate the interaction volume crossing a grain boundary so that the effect on the accuracy of the cross correlation results can be tested. It was found that the accuracy of HR-EBSD strain measurements performed in a FEG-SEM on zirconium remains good until the incident beam is less than 18 nm from a grain boundary. A simulated microstructure was used to measure how often pattern overlap occurs at any given EBSD step size, and a simple relation was found linking the probability of overlap with step size.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultramicroscopy - Volume 155, August 2015, Pages 62-73
نویسندگان
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