کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
8038172 1518328 2015 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Vibrational and optical spectroscopies integrated with environmental transmission electron microscopy
ترجمه فارسی عنوان
طیف سنجی ارتعاشی و نوری با میکروسکوپ الکترونی انتقال محیطی
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
چکیده انگلیسی
Here, we present a measurement platform for collecting multiple types of spectroscopy data during high-resolution environmental transmission electron microscopy observations of dynamic processes. Such coupled measurements are made possible by a broadband, high-efficiency, free-space optical system. The critical element of the system is a parabolic mirror, inserted using an independent hollow rod and placed below the sample holder which can focus a light on the sample and/or collect the optical response. We demonstrate the versatility of this optical setup by using it to combine in situ atomic-scale electron microscopy observations with Raman spectroscopy. The Raman data is also used to measure the local temperature of the observed sample area. Other applications include, but are not limited to: cathodo- and photoluminescence spectroscopy, and use of the laser as a local, high-rate heating source.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultramicroscopy - Volume 150, March 2015, Pages 10-15
نویسندگان
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