کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
96406 | 160462 | 2012 | 5 صفحه PDF | دانلود رایگان |
The results of the analysis of some herbal products and powders adulterated with alkylindoles recovered on the Italian market between 2010 and 2011 are reported. Besides the well-known alkyindoles JWH-018 and JWH-073, other derivatives such as JWH-250 and AM-694 have been detected and for the first time in Italy 1-butyl-3-(1-(4-methyl)naphthoyl)indole (compound 1), the 4-methylnaphthoyl analogue of JWH-073. This compound as well as the other alkylindoles has been synthesized and characterized by 1H NMR, 13C NMR, DSC, GC/MS, and elemental analysis.The quantitative analyses of the samples have been carried out by means of the GC/FID method developed in our laboratory for the analysis of herbal high products containing naphthoylindoles; the quantity of the cannabimimetic substances ranged from 6 mg/g to 47 mg/g.
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► GC/MS and GC/FID analysis of herbal high products seized in Italy in 2010–2011.
► Adulteration of these herbal products with illegal alkylindoles.
► Identification of 1-butyl-3-(1-(4-methyl)naphtoyl)indole for the first time in Italy.
Journal: Forensic Science International - Volume 223, Issues 1–3, 30 November 2012, Pages e42–e46