کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9829434 | 1524491 | 2005 | 9 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
CTAB assisted one-pot hydrothermal synthesis of columnar hexagonal-shaped ZnO crystals
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
فیزیک و نجوم
فیزیک ماده چگال
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: CTAB assisted one-pot hydrothermal synthesis of columnar hexagonal-shaped ZnO crystals CTAB assisted one-pot hydrothermal synthesis of columnar hexagonal-shaped ZnO crystals](/preview/png/9829434.png)
چکیده انگلیسی
In the current paper, we report the preparation of micron sized hexagonal-shaped ZnO crystals having a stepped columnar structure using a cetyltrimethylammonium bromide (CTAB)-assisted hydrothermal synthesis route. ZnAc2·2H2O and KOH were used as the starting materials and zinc oxide crystals were obtained following growth at 120 °C for 5 h. Experimental results showed that the presence of CTAB in the system could vary the shape of the ZnO crystals: some rod-shaped ZnO crystals were prepared from the system without CTAB and stepped hexagonal-shaped ZnO crystals were produced from the system with CTAB. The morphology of the final product could also be influenced by the molar ratio of ZnAc2/KOH in the system. The lower concentration of KOH availed the formation of stepped hexagonal shaped ZnO crystals. Furthermore, many nanorods were obtained when ZnCl2 was used as a zinc ion source, which implied that the counter anion in the system could affect the morphology of the final product. A possible formation process of the ZnO crystals was suggested.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Crystal Growth - Volume 283, Issues 1â2, 15 September 2005, Pages 48-56
Journal: Journal of Crystal Growth - Volume 283, Issues 1â2, 15 September 2005, Pages 48-56
نویسندگان
Yong-Hong Ni, Xian-Wen Wei, Xiang Ma, Jian-Ming Hong,