کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10556873 | 968435 | 2011 | 9 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Development, validation and application of Micellar Electrokinetic Capillary Chromatography method for routine analysis of catechins, quercetin and thymol in natural samples
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کلمات کلیدی
(−)-gallocatechin gallateMEKCCMC(−)-catechin gallateEGCGCatechinsEGCGCG(−)-epicatechin - (-) - epicatechin(−)-epicatechin gallate - (-) - Epicatechin گالات(−)-epigallocatechin - (-) - epigallocatechin(−)-epigallocatechin gallate - (-) - epigallocatechin گالاتAntioxidants - آنتی اکسیدانECG - الکتروکاردیوگرام یا نوار قلبQUER - بخواهیPolyphenolic compounds - ترکیبات پلیفنیکThy - توthymol - تیمولCritical micellar concentration - غلظت میکرولیکی بحرانیQuercetin - کوئرستین
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Development, validation and application of Micellar Electrokinetic Capillary Chromatography method for routine analysis of catechins, quercetin and thymol in natural samples Development, validation and application of Micellar Electrokinetic Capillary Chromatography method for routine analysis of catechins, quercetin and thymol in natural samples](/preview/png/10556873.png)
چکیده انگلیسی
Natural matrices such as several vegetables, fruits or beverages are the origin of different natural antioxidants with great interest to be used instead of synthetic antioxidants in several applications, as a result of their health-promoting and disease-preventing properties. In this work, a capillary electrophoresis method capable of separating and quantifying some of these antioxidants (seven catechins with the same or similar molecular weight and relation q/z) is showed. Short analysis time and precision parameters equivalent to those obtained by liquid chromatography were obtained. This method was developed using the micellar electrokinetic chromatography (MEKC) mode with ultraviolet-visible detection. Quality parameters were established, obtaining low instrumental detection and quantification limits (0.6-2.0 mg Lâ 1 and 2.0-6.5 mg Lâ 1, respectively), good precision (relative standard deviation in the intermediate repeatability lower than 7% for every compound) and short analysis time. The developed method also showed good performance for the determination of two more natural antioxidants, quercetin and thymol. The applicability of the method to the analysis of catechins in several natural samples was tested.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Microchemical Journal - Volume 99, Issue 2, November 2011, Pages 461-469
Journal: Microchemical Journal - Volume 99, Issue 2, November 2011, Pages 461-469
نویسندگان
MarÃa del Mar Castro López, José M. López Vilariño, MarÃa Victoria González RodrÃguez, LuÃs F. Barral Losada,