کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10560085 | 969703 | 2005 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Analysis of earthy and musty odors in water samples by solid-phase microextraction coupled with gas chromatography/ion trap mass spectrometry
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A method for the determination of the earthy and musty odors geosmin, 2-methylisoborneol (2-MIB), 2-isobutyl-3-methoxy pyrazine (IBMP), 2-isopropyl-3-methoxy pyrazine (IPMP) and 2,4,6-trichloroanisole (2,4,6-TCA) in water by headspace solid-phase microextraction (HSSPME) combined with gas chromatography-ion trap mass spectrometry (GC-ITMS) is described. Several parameters of the extraction and desorption procedure were studied and optimized (such as types of fibers, extraction temperature, extraction time, desorption temperature, desorption time, ionic strength and elutropic strength and pH of samples). The method shows good linearity over the concentration range 1-500 ng lâ1 and gives detection limits of sub-part per trillion levels for all compounds. Good precision (5.9-9.8%) is obtained using IBMP as internal standard. Finally, the method was successfully applied to analyze earthy and musty odors in tap water and lake water.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Talanta - Volume 65, Issue 2, 30 January 2005, Pages 518-524
Journal: Talanta - Volume 65, Issue 2, 30 January 2005, Pages 518-524
نویسندگان
Yu-Hsiang Sung, Tzu-Ying Li, Shang-Da Huang,