کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1180088 | 1491482 | 2016 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis, crystal and molecular structure, Hirshfeld surface analysis of diethyl 2-(4-methylbenzylidene)malonate
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Synthesis, crystal and molecular structure, Hirshfeld surface analysis of diethyl 2-(4-methylbenzylidene)malonate Synthesis, crystal and molecular structure, Hirshfeld surface analysis of diethyl 2-(4-methylbenzylidene)malonate](/preview/png/1180088.png)
چکیده انگلیسی
Diethyl 2-(4-methylbenzylidene)malonate was synthesized by Knoevenagel condensation reaction of 4-methylbenzaldehyde and diethyl malonate in the presence of catalytic amount of piperidine and trifluoroacetic acid in benzene under reflux conditions. The product obtained was characterized by 1H NMR, Mass spectroscopy and by X-ray diffraction studies. The title compound C15H18O4 crystallizes in the monoclinic crystal system with space group C2/c and unit cell parameters, a = 18.210(4) Å, b = 8.316(2) Å, c = 20.130(4) Å, β = 109.0(2)° and Z = 8. The crystal and molecular structure of the title compound is stabilized by CH ···O hydrogen bond interactions.
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ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Chemical Data Collections - Volume 2, May 2016, Pages 17–24
Journal: Chemical Data Collections - Volume 2, May 2016, Pages 17–24
نویسندگان
Dileep Kumar Achutha, Prabhuswamy Mallappa, Lokanath Neratur Krishnappagowda, Ajay Kumar Kariyappa,