کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1220458 | 1494641 | 2014 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Separation and structural elucidation of a new tadalafil analogue diethylaminopretadalafil included as an adulterant in a dietary supplement
ترجمه فارسی عنوان
جداسازی و تشریح ساختاری یک آنالوگ تادالافیل جدید دیاتیلامینوپرتادالافیل شامل یک مخلوط کننده در یک مکمل رژیم غذایی
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
چکیده انگلیسی
• In the present study, a new tadalafil analogue as an adulterant in a dietary supplement was detected and isolated.
• The structure of the new analogue was elucidated by means of NMR, HPLC and mass spectroscopy.
• The possible origination of the new analogue was also proposed here.
• The structure of this analogue was identified and reported for the first time.
A new tadalafil analogue was detected and isolated from a dietary supplement, the structure was elucidated by means of nuclear magnetic resonance (NMR) and mass spectroscopy. The compound was determined to be diethylaminopretadalafil, which might be derived from a precursor in the synthesis of tadalafil.
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ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Pharmaceutical and Biomedical Analysis - Volume 94, June 2014, Pages 210–214
Journal: Journal of Pharmaceutical and Biomedical Analysis - Volume 94, June 2014, Pages 210–214
نویسندگان
Gaofei Zhang, Yue Yu, Xiaoou Wu, Jun Li,