کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1385883 982461 2006 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Complete 1H and 13C NMR assignment of digeneaside, a low-molecular-mass carbohydrate produced by red seaweeds
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آلی
پیش نمایش صفحه اول مقاله
Complete 1H and 13C NMR assignment of digeneaside, a low-molecular-mass carbohydrate produced by red seaweeds
چکیده انگلیسی

Digeneaside (α-d-mannopyranosyl-(1→2)-d-glycerate) was extracted from the red algae, Bostrychia binderii, and purified by adsorption and gel-filtration chromatography. HPLC and ESI-MS techniques were used to follow purification steps and characterize digeneaside. NMR spectroscopy experiments (1D 1H, 13C, DEPT and 2D HMQC, COSY and TOCSY) were used to fully assign the 1H and 13C spectra.

Digeneaside (α-d-Manp-(1→2)-d-glycerate) was extracted from the red algae, Bostrychia binderii. HPLC and ESI-MS techniques were used to characterize the glycoside. NMR experiments (1D 1H, 13C, DEPT and 2D HMQC, COSY and TOCSY) were used to fully assign the 1H and 13C spectra.Figure optionsDownload as PowerPoint slide

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Research - Volume 341, Issue 5, 10 April 2006, Pages 677–682
نویسندگان
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