کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1385883 | 982461 | 2006 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Complete 1H and 13C NMR assignment of digeneaside, a low-molecular-mass carbohydrate produced by red seaweeds
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
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چکیده انگلیسی
Digeneaside (α-d-mannopyranosyl-(1→2)-d-glycerate) was extracted from the red algae, Bostrychia binderii, and purified by adsorption and gel-filtration chromatography. HPLC and ESI-MS techniques were used to follow purification steps and characterize digeneaside. NMR spectroscopy experiments (1D 1H, 13C, DEPT and 2D HMQC, COSY and TOCSY) were used to fully assign the 1H and 13C spectra.
Digeneaside (α-d-Manp-(1→2)-d-glycerate) was extracted from the red algae, Bostrychia binderii. HPLC and ESI-MS techniques were used to characterize the glycoside. NMR experiments (1D 1H, 13C, DEPT and 2D HMQC, COSY and TOCSY) were used to fully assign the 1H and 13C spectra.Figure optionsDownload as PowerPoint slide
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Research - Volume 341, Issue 5, 10 April 2006, Pages 677–682
Journal: Carbohydrate Research - Volume 341, Issue 5, 10 April 2006, Pages 677–682
نویسندگان
Sérgio D. Ascêncio, Alexandre Orsato, Robson A. França, M. Eugênia R. Duarte, Miguel D. Noseda,