کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1623856 | 1516417 | 2008 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
The crystal structure of LiMgAlD6 from combined neutron and synchrotron X-ray powder diffraction
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فلزات و آلیاژها
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: The crystal structure of LiMgAlD6 from combined neutron and synchrotron X-ray powder diffraction The crystal structure of LiMgAlD6 from combined neutron and synchrotron X-ray powder diffraction](/preview/png/1623856.png)
چکیده انگلیسی
LiMgAlH6 is the intermediate phase when LiMg(AlH4)3 is heated. It contains 9.4 wt.% hydrogen, of which 4.8 wt.% is released during the decomposition step to MgH2 and LiH. Deuterated LiMgAlD6 was prepared by heat-treating LiMg(AlD4)3 at 130 °C. Powder neutron and synchrotron X-ray diffraction patterns were measured and the structure was refined using the Rietveld technique on both patterns simultaneously. LiMgAlD6 crystallizes in the trigonal space group P321 with a = 7.9856(4) Å and c = 4.3789(3) Å. The structure consists of isolated AlD6 octahedra connected through octahedrally coordinated Mg- and Li-atoms.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Alloys and Compounds - Volume 460, Issues 1–2, 28 July 2008, Pages 64–68
Journal: Journal of Alloys and Compounds - Volume 460, Issues 1–2, 28 July 2008, Pages 64–68
نویسندگان
Hilde Grove, Hendrik W. Brinks, Ole M. Løvvik, Richard H. Heyn, Bjørn C. Hauback,